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Th e soone r th e issu e of catalys t pric e is understoo d th e bette r it is for all parties . Th e invento r shoul d als o seek at thi s tim e a commitmen t fro m th e custo m manufacture r as t o th e cost of th e scale-u p program , sinc e man y vendor s expec t thes e cost s t o b e born e b y th e invento r even if commercial-scal e manufactur e is neve r realized . 2 Catalyst Scale-up—Pitfall or Payoff? 35 Fig. 2. Typical glass-lined pilot plant system for precipitating catalyst formulations in a corrosive environment.

Charles N. Satterfield, CHEMTECH 11, 618-624, October (1981). A. , Thomas, and C. P. Brundrett, Chem. Eng. Prog. 76, 4 1 - 4 5 , June (1980). David L. Trimm, CHEMTECH % 571-577, September (1979). Sol W. Weller, AIChE Symp. Ser. 70, 143 (1974). "Catalyst Handbook" Wolfe Scientific Books, London (1970). CHAPTER 3 Laborator y Reactor s for Catalyti c Studie s J . M. B E R T Y * Berty Reaction Engineers, Ltd. Erie, Pennsylvania I. II. III. IV. V. VI. VII. Introduction The Purpose of Laboratory Reactors A.

The Loop or Recycle Reactor C. Construction Concepts for Gradientless Reactors . . Conclusion References 42 43 43 44 46 46 47 48 48 50 52 52 53 54 54 56 60 60 61 63 66 66 Notation s 2 a A C c p D 2 Transfer area (m ) Flow cross section (m )3 Concentration (mol/m ) Heat capacity 2(kJ/kg K) Diffusivity (m /sec) * Present address: Department of Chemical Engineering, University of Akron, Akron, Ohio, 44325. Applie d Industria l Catalysi s Volum e 1 41 Copyrigh t ' 1983 Academi c Press , Inc . All rights of reproductio n in an y form reserved .

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